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Bew, Sean P. 
ORCID: https://orcid.org/0000-0002-9087-9463, Brimage, Rebecca A., Hughes, David L., Legentil, Laurent, Sharma, Sunil V. and Wilson, Martin A.
(2007)
Expedient synthesis of substituted (diphenylphosphinoylmethyl)benzenes.
The Journal of Organic Chemistry, 72 (7).
pp. 2655-2658.
Abstract
An efficient protocol for the synthesis of structurally diverse (diphenylphosphinoylmethyl)benzenes is described. The reaction employs readily available carboxylic acids, chlorodiphenylphosphine, and water as the reagents. A 97% reduction in the reaction times and substantially higher yields of products result, up to a 60% increase, if the reactions are performed under microwave irradiation. The first examples of transition-metal-catalyzed reactions applied to 4-bromo-1,3-bis(diphenylphosphinoylmethyl)benzene are also reported. © 2007 American Chemical Society.
| Item Type: | Article |
|---|---|
| Faculty \ School: | Faculty of Science > School of Chemistry (former - to 2024) Faculty of Science > School of Chemical Sciences and Pharmacy (former - to 2009) |
| UEA Research Groups: | Faculty of Science > Research Groups > Chemistry of Materials and Catalysis Faculty of Science > Research Groups > Synthetic Chemistry (former - to 2017) |
| Related URLs: | |
| Depositing User: | Rachel Smith |
| Date Deposited: | 15 Feb 2011 10:07 |
| Last Modified: | 24 Sep 2024 09:38 |
| URI: | https://ueaeprints.uea.ac.uk/id/eprint/21371 |
| DOI: | 10.1021/jo062114k |
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