In Situ Sulfidation of Pd/C: A Straightforward Method for Chemoselective Conjugate Reduction by Continuous Hydrogenation

Moore, Jonathan C., Howie, Rowena A., Bourne, Samuel L., Jenkins, Gareth N., Licence, Peter ORCID: https://orcid.org/0000-0003-2992-0153, Poliakoff, Martyn and George, Michael W. (2019) In Situ Sulfidation of Pd/C: A Straightforward Method for Chemoselective Conjugate Reduction by Continuous Hydrogenation. ACS Sustainable Chemistry & Engineering, 7 (19).

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Abstract

A method has been developed for the in situ sulfidation of Pd/C under continuous flow. The approach provides a cheap, sustainable, and operationally convenient method for chemoselective conjugate reduction by continuous hydrogenation. High conversions and excellent selectivities were obtained for olefin reduction in α/β-unsaturated carbonyl compounds in the presence of hydrogenatively sensitive functionalities. The methodology was analyzed with a green metric system to highlight the sustainability features of the process.

Item Type:	Article
Faculty \ School:	Faculty of Science > School of Chemistry, Pharmacy and Pharmacology
Related URLs:	https://doi.org/10.1021/acssuschemeng.9b...
Depositing User:	LivePure Connector
Date Deposited:	01 Oct 2026 10:27
Last Modified:	06 Oct 2026 23:25
URI:	https://ueaeprints.uea.ac.uk/id/eprint/104700
DOI:	10.1021/acssuschemeng.9b04347

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